Diazotisation Titration Notes Pdf Free Download

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Diazotization is used in the analysis of aromatic compounds containing an amino group in the molecules. This analysis is based on the reaction between aromatic primary amine (–NH2), and HONO, in presence of excess mineral or inorganic acids.

NaNO2 is generally used in the direct method of diazotization. It gives HNO2 in an acidic solution. Many aromatic primary amines with free –NH2 groups can be analyzed quantitatively by measuring the volume of NaNO2 solution required to convert them into diazonium salts.

The typical reaction of diazotization reaction in presence of HCl is given as:
NaNO2 + HCl -----> HONO + NaCl
ArNH2 + HONO + HCl ArN2Cl + 2H2O

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Diazotisation Titration Notes Pdf Includes Topics

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  • Condition for diazotization
  • Rate of titration
  • Temperature
  • The visual endpoint determination method
  • Electrometric End Point determination method
  • Application of diazotization titration

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