Practical Lab Manual of Pharmaceutical Inorganic and Analytical Chemistry – BP111P Bachelor of Pharmacy (B.Pharm) 1st Semester As per NEP 2020, New Detailed Syllabus wise all practical details.
- Limit tests (Any 4 Experiments)
a. Limit test and modified limit test for Chloride as per Indian Pharmacopoeia
b. Limit test and modified limit test for sulphate as per Indian Pharmacopoeia
c. Limit test for Iron
d. Limit test for Lead
e. Limit test for arsenic - Preparation of inorganic pharmaceuticals (Any 3 Experiments)
a. Preparation of Aluminium hydroxide
b. Preparation of potash alum
c. Preparation of ferrous sulphate
d. Preparation of Magnesium sulphate from magnesium hydroxide or magnesium carbonate - Test for Purity (Any 2 Experiments)
a. Assessment of swelling power of bentonite as per Indian Pharmacopoeia
b. Evaluation of acid neutralizing capacity of aluminium hydroxide gel
c. Determination of potassium iodate and iodine in potassium Iodide - Assay of the following inorganic compounds including standardization of titrant (Any 5 Experiments)
a. Assay of ammonium chloride by acid base titration,
b. Assay of Ferrous sulphate by Cerimetry,
c. Assay of Copper sulphate by Iodometry,
d. Assay of Calcium gluconate by Complexometry,
e . Assay of Hydrogen peroxide byPermanganometry,
f. Assay of Sodium benzoate by non-aqueous titration, g. Assay of Sodium Chloride by precipitation titration (Modified Volhard’s method)
Recommended References (Preferably latest editions)
- Bentley, R. and Driver, J., Bentley and Driver’s Textbook of Pharmaceutical Chemistry. Oxford: Oxford University Press.
- Vogel, A.I., Vogel’s Textbook of Quantitative Chemical Analysis. Essex: Pearson Education Limited.
- Beckett, A.H. and Stenlake, J.B., Practical Pharmaceutical Chemistry. Part I & II. London: The Athlone Press, University of London.
- Kennedy, J.H., Analytical Chemistry: Principles. New York: Saunders College Publishing.
- Schroff, M.L., Inorganic Pharmaceutical Chemistry. New Delhi: Oxford Book Company.
- Indian Pharmacopoeia Commission, Indian Pharmacopoeia. Ghaziabad, India.